PHARMACEUTICAL ANALYSIS QUESTION BANK FOR B.PHARMACY 1 SEMESTER

PHARMACEUTICAL ANALYSIS

UNIT-1

Introduction of Pharmaceutical Analysis

QUESTIONS FROM THE ABOVE TOPIC

Short Answer Questions (4 marks)

1. Define Pharmaceutical analysis & discuss about their Scopes.

2. Write short notes on Techniques pharmaceutical analysis,

3. Write short notes on

i. Primary standards

ii. Secondary standards

iii. Volumetric Methods

4. Write short notes on

i. Percent Concentration

ii. Molar Concentration

iii. Parts per Million and Parts per Billion

5. Preparation and Standardization of Sulphuric Acid

Pharmaceutical Errors

Short Answer Questions (4 marks)

1 Define Pharmaceutical Errors& discuss about Indeterminate error

2. Write short notes on indeterminate error.

3. Write short notes on

i. Significant figures

ii. Rounding off figures

4. What is Accuracy and Precision ?

5. Write in brief Source and type of errors

Pharmacopoeia, Sources of impurities & Limit test

Short Answer Questions (4 marks)

1. Define Pharmacopeia & discuss about latest edition.

2. Write short notes on Indian Pharmacopeia.

3. Write about Sources of impurities

4. Write short notes on

i. Limit test of arsenic

ii. Limit test of heavy metals

5. How you can minimize Pharmaceutical impurities ?

6. Write in brief Limit test Discuss anyone.

UNIT-2

Acid-Base Titration, Types of acid base titration, Non-aqueous titration

Short Answer Questions (4 marks)

1. Define Buffer solution, mixed indicators, Acid & Base

2. Write short notes on Types of acid base titration.

3. Write about Estimation of Sodium Benzoate

4. Write short notes on (Any 2)

i. Leveling effect

ii. Selection of solvent

iii. Types of solvents in non-aqueous titrations

iv. Acidimetry and Alkalimeter titration

5. Write about Theories of Acid-base Titration ?

6. Write in brief Indicators of Acid Base Titrations.

7. Explain Law of mass action in details.

8. What is Common ion effect

UNIT-3

Precipitation titration, Complexometric titration, Gravimetric diazotization titration

UNIT-4

Redox Titration

Short Answer Questions (4 marks)

1. Define Redox Titration& discuss about DICHROMETRY

2. Write short notes on lodimetry And lodometry.

3. Write about Redox Indicators.

4. Write short notes on

i. Some common oxidants and reductants

ii. Theory of redox titrations

4. Explain Concept of oxidation and reduction

5. Write in brief Oxidation Number or Oxidation State.

UNIT-5

Electrochemical methods, Potentiomeiy & Polarography

Short Answer Questions (4 marks)

1. What is electrometric method explain rotating platinum electrode

2. Write short notes on Paleography

3. Write about Standard Hydrogen Electrode (SHE).

4. Write short notes on

i. Saturated calomel electrode (SCE)

ii. Silver Chloride (Ag-AgCI)electrode

iii. Advantages of DME

5. Explain Concept of glass electrode

6. Write in brief applications and advantages of potentiometric titrations